By Klaus Bauer, Gilbrecht Haller (auth.)
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Extra resources for Compounds of Transition Metals
Chemical fixation of molecular N2 (2413, 2414). N2 fixation of systems cP2TiC12-RMgX, R = Et, Pr, i-Bu; X = Br (2415). N2 insertion into the metal-carbon bond in the presence of PhLi (2417) • Lability of the Ti-Cl bond by exchange rxn. between cp2TiC12 and 36Cl-labeled LiCl in solvents of different DK at 0-25° (2086). Thermochemical data (2289). 20 and in HCONMe2 (2386). Determination of the ratio H/cP2TiC12 either for hydrogenation or polymn. of styrene (2155). Investigation of the catalytic activity for C2H4 polymn.
From cP2TiC12 with Br2 (266). : Effects of substituents on NMR spectrum (1722). : Effects of substituents on NMR spectrum (1722). : From MeCsH4Ti(OEt)2 with AcCl (1734). : m. 98-99° (674, 1734), IR spectrum (1734), effects of substituents on NMR spectrum (1722). Rxn. with: MeCsH4Ti(OEt)s ~ MeCsH4Ti(OEt)2C1 or MeCsH4Ti(OEt)C12 (1734). t. (1734). : Orange crystals which liquify in air, sub1l 136° (1734), b l 136°, IR (674) and NMR (1690) spectra. : By heating a suspension of MesCsLi in CaRs with TiC14, 15% yield (1256).
Rxn. with: MeTi(O-i-Pr)s ~ MeTi(O-i-Pr)2Cl and MeTi(O-i-Pr)C12 (443). ~: Polymn. catalyst (ethylene, propylene) (~~). : By rxn. of TiC~ with MeMgI, followed by C10HeN2 (2294). : Red-violet (2294). : Calcn. of the electronic energy levels (156). EtTiCls Dichlorodiethyltitanium (M-8) Rxn. with: EtOH ~ Et2Ti(OEt)Cl (1171). Use: In combination with Me2AlCl a polymn. catalyst, detn. of the rates of polymn. of C2H4 and C2D4 (948). Effect on the polymn. activity in combination with ReAl or R2AlCl (1171).
Compounds of Transition Metals by Klaus Bauer, Gilbrecht Haller (auth.)